Construction materials. Values ​​of critical heat flux density Value of critical surface heat flux density

The method belongs to large-scale, which is associated with the size of the installation (shaft furnace) and samples of the test material.

It is used to test all homogeneous and layered combustible materials, including those used as finishing and facing, as well as paint and varnish coatings.

The essence of the method consists in exposing the material sample to the flame of a gas burner for 10 min and recording the parameters characterizing its behavior during fire exposure.

12 samples. Sample sizes: 1000x190 mm, up to 70 mm thick. they are arranged vertically, stacking 4 in the form of a box.

The test facility is a vertical shaft furnace.

The sequence of operations in the testing process is as follows.

    Weigh samples and attach them to the holder frame 4.

    Insert samples 6 into the combustion chamber 9, secure and close the door 5.

    Turn on the fan 13 (turning on the fan is the beginning of the test).

    Ignite the gas burner 10.

    From the moment the tests begin, the temperature of the flue gases is recorded for 10 minutes using thermocouples. 8 and self-burning time of the sample.

    After testing, the cooled samples are removed from the furnace, the length of the damaged part of the samples is measured and weighed.

The test results are evaluated according to table. 1.5.

Table 1.5

Classification of materials by flammability groups

Group

combustibility

materials

Flammability parameters

Flue gas temperature /,°C

Degree of damage along the lengthSi, %

Degree of damage by weightSu, %

Duration of independent COMBUSTION 1sg,With

Note. For materials of combustibility groups G1-GZ, the formation of burning melt drops during testing is not allowed.

  1. Method for testing materials for flammability

. The method is applied to all homogeneous and layered combustible building materials.

The essence of the method is to determine the flammability parameters of the material at given standard levels of exposure to the sample surface of the radiant heat flux and flame from the ignition source, which are determined on the device shown in Fig. 1.8.

Flammability parameters are KPPTP - critical surface heat flux density and ignition time.

KPPTP - the minimum value of the surface heat flux density (PPTP), at which a stable

fiery combustion. KPPTP is used to classify materials into flammability groups.

Levels of exposure to radiant heat flux should be in the range from 5 to 50 kW/m 2 .

For testing, 15 samples are prepared, having the shape of a square with a side of 165 (-5) mm, with a thickness of not more than 70 mm.

The test order is as follows.

    After conditioning, the sample is wrapped in a sheet of aluminum foil, in the center of which a hole with a diameter of 140 mm is cut.

    The power supply is turned off and the value of thermo-EMF (voltage) obtained during the calibration of the installation, corresponding to PPTP 30 kW/m 2, is set using the regulating thermoelectric converter (thermocouple).

    After reaching the set thermo-EMF value, the installation is kept in this mode for at least 5 minutes. In this case, the thermo-EMF value should not deviate by more than 1%.

    Place the shield plate on the protective plate, replace the dummy piece with the test piece, turn on the movable burner mechanism, remove the shield plate, and turn on the time recorder.

    After 15 min or when the specimen ignites, the test is terminated. To do this, place the shielding plate on the protective plate, stop the time recorder and the mechanism of the movable burner, remove the holder with the sample and place the imitator sample on the movable platform, remove the shielding plate.

    Set the value of PPTP 20 kW / m 2 (if ignition was recorded in the previous test) or 40 kW / m 2 in its absence. Repeat the operations according to paragraphs 5-7.

    If ignition is detected at PPTP 20 kW/m 2 , reduce the PPTP value to 10 kW/m 2 and repeat steps 5-7.

    If there is no ignition at TPTP 40 kW/m 2 , set the TPTP value to 50 kW/m 2 and repeat steps 5-7. If there is no ignition at 50 kW/m 2 APRT, 2 more tests are carried out at this APRT, and if ignition is not observed, then the tests are stopped.

11. After determining two values ​​of PPTP, with one of which ignition is observed, while the other is absent, set the value of PPTP by 5 kW / m 2 more than the value at which there is no ignition, and repeat steps 5-7 on three samples.

For KPPTP consider the smallest value of PPTP, at which ignition is recorded for sin samples.

The flammability of materials is assessed

    Flame Propagation Test Method for Materials

The method is applicable to all homogeneous and layered combustible materials used in the surface layers of floors and roofs of buildings.

The essence of the method is to determine the critical surface heat flux density (CCTF), the value of which is set along the length of the flame propagation along the sample as a result of the heat flux acting on its surface.

Flame propagation length (I) - the maximum amount of damage to the surface of the sample as a result of the propagation of flame combustion.

For testing, 5 samples of material with a size of 1100 x 250 mm are made. For anisotropic materials, 2 sets of samples are made (for example, weft and warp). Samples are made in combination with a non-combustible base. The method of attaching the material to the base must correspond to that used in real conditions. As a non-combustible base, asbestos-cement sheets with a thickness of 10 or 12 mm are used. The thickness of the sample with a non-combustible base should be no more than 60 mm.

The test setup consists of the following main

test chamber with chimney and exhaust hood;

source of radiant heat flux (radiation panel);

source of ignition (gas burner);

sample holder and a device for inserting the holder into the test chamber (platforms).

The installation is equipped with instruments for recording and measuring the temperature in the test chamber and chimney.

The test order is as follows.

    After calibration of the installation, i.e. after establishing the PPTP values ​​required by GOST at the given points of the calibration sample and along its surface, as well as preparing it for operation, open the chamber door and light the gas burner, positioning it so that the distance to the exposed surface is at least 50 mm.

    Install the sample in the holder, fix it, place it on the platform and introduce it into the chamber.

    Close the chamber door and start the stopwatch. After holding for 2 minutes, the burner flame is brought into contact with the sample at the point

    located on the central axis. Leave the flame in this position for 10 minutes. After the time has elapsed, the burner is returned to its original position.

    If the sample does not ignite within 10 min, the test is considered to be completed. If the specimen ignites, the test is terminated when the flame ceases to burn or after 30 min.

the sample is carried out after the sample holder is cooled to room temperature and the compliance of the PPTP with the requirements of GOST is checked.

    Measure the length of the damaged part of the sample along its longitudinal axis for each of the five samples.

Damage is considered to be burnout and charring of the sample material as a result of the spread of fiery combustion over its surface. Melting, warping, sintering, swelling, shrinkage, change in color, shape, violation of the integrity of the sample (tears, surface chips) are not considered damage.

The length of flame propagation is determined as the arithmetic mean of the length of the damaged part of the five samples.

Combustible building materials, depending on the size of the KPPTP, are divided into 4 groups of flame propagation

INTERSTATE SCIENTIFIC AND TECHNICAL COMMISSION FOR STANDARDIZATION, TECHNICAL REGULATION AND CERTIFICATION IN CONSTRUCTION

BUILDING MATERIALS

Flammability test method

BUILDING MATERIALS
Ignitability Test Method

Introduction date 1996-07-01

Content
Introduction
1 area of ​​use
2 Normative references
3 Definitions
4 Fundamentals
5 Classification of building materials according to flammability groups
6 Test specimens
7 Test equipment
8 Installation calibration
9 Testing
10 Test report
11 Requirements
Annex A (informative)

Foreword

1. DEVELOPED by the State Central Research and Design and Experimental Institute of Complex Problems of Building Structures and Structures named after V.A. Kucherenko (TsNIISK named after Kucherenko) of the State Scientific Center "Construction" (SSC "Construction") of the Ministry of Construction of Russia together with the All-Russian Research Institute of Fire Defense () of the Ministry of Internal Affairs of Russia and the Center for Fire Research and Thermal Protection in Construction TsNIISK (TsPITZS TsNIISK)
INTRODUCED by the Ministry of Construction of Russia
2. ADOPTED by the Interstate Scientific and Technical Commission for Standardization, Technical Regulation and Certification in Construction (MNTKS) on May 15, 1996.
voted to accept
State name Name of the public administration body for construction
The Republic of Azerbaijan Gosstroy of the Republic of Azerbaijan
Republic of Armenia State Architecture of the Republic of Armenia
The Republic of Moldova Ministry of Architecture of the Republic of Moldova
the Russian Federation Ministry of Construction of Russia
The Republic of Tajikistan Gosstroy of the Republic of Tajikistan
The Republic of Uzbekistan Goskomarchitektstroy of the Republic of Uzbekistan


3. INTRODUCED FOR THE FIRST TIME
4. INTRODUCED from 07/01/96 as the state standard of the Russian Federation by the Decree of the Ministry of Construction of Russia dated 06/24/96 N 18-40.

Introduction

developed on the basis of ISO 5657-86 "Fire tests - reaction to fire - flammability of building structures". The standard uses the fundamental provisions for determining the ability to ignite building products with simultaneous exposure to radiant heat flux and an open flame from an ignition source. The test equipment is identical to the equipment recommended in the ISO standard.

1 area of ​​use

This International Standard specifies a method for testing building materials for flammability and classifying them into flammability groups.
This International Standard applies to all homogeneous and layered combustible building materials.

2. Regulatory references

References are made to the following regulatory documents:
;
;
GOST 18124-95 Flat asbestos-cement sheets;

.

3. Definitions

This standard uses the terms and definitions according to ST SEV 383, as well as the following terms with the corresponding definitions:
3.1. Flammability- the ability of substances and materials to ignite.
3.2. Ignition— initiation of flame combustion under the influence of an ignition source, in this standard test, it is characterized by stable flame combustion.
3.3. Ignition time is the time from the start of the test to the onset of sustained flame combustion.
3.4. Sustainable flame burning- burning, continuing until the next exposure to the flame sample from the ignition source.
3.5. Surface heat flux density(PPTP) - radiant heat flux acting on a unit surface of the sample.
3.6. Critical surface heat flux density(KPPTP) - the minimum value of the surface heat flux density at which stable flame combustion occurs.
3.7. exposed surface- the surface of the sample exposed to radiant heat flux and flame from an ignition source during the flammability test.

4. Basic provisions

4.1. The essence of the method is to determine the flammability parameters of the material at the levels of exposure to the surface of the sample of radiant heat flux and flame from the ignition source specified by the standard.
The flammability parameters of the material are the KPPTP and the ignition time.
To classify materials according to flammability groups, KPPTP is used.
4.2. The radiant heat flux density should be in the range from 10 to 50 kW/m².
4.3. The initial radiant heat flux density during testing (RTF) is 30 kW/m².

5. Classification of building materials according to flammability groups

5.1. Combustible building materials (according to GOST 30244), depending on the size of the KPPTP, are divided into three flammability groups: B1, B2, B3 (table 1).

Table 1

6. Samples for testing

6.1. For testing, 15 samples are made, having the shape of a square, with a side of 165 mm and a deviation of minus 5 mm. The thickness of the samples should be no more than 70 mm. At each value of PPTP, the tests are carried out on three samples.
6.2. During the preparation of samples, the exposed surface should not be processed.
If there are corrugations, relief, embossing, etc. on the exposed surface. the size of the protrusions (cavities) should be no more than 5 mm.
If the exposed surface does not meet the specified requirements, it is allowed to make samples for testing from a material with a flat surface, i.e. without corrugations, relief, embossing, etc.
6.3. Samples for standard testing of materials used only as finishing and facing, as well as for testing paint and varnish coatings and roofing materials, are made in combination with a non-combustible base. The fastening method must ensure close contact between the surfaces of the material and the base.
As a non-combustible base, asbestos-cement sheets according to GOST 18124 with a thickness of 10 or 12 mm should be used.
In cases where the specific technical documentation does not provide conditions for a standard test, the samples are made with the base and fastening specified in the technical documentation.
6.4. Paint and varnish coatings, as well as roofing mastics, should be applied to the base in at least four layers, while the consumption of material when applied to the base of each layer should correspond to that adopted in the technical documentation.
6.5. For materials used both independently (for example, for structures) and as finishing and facing materials, samples must be made in accordance with 6.1 (one set) and 6.3 (one set).
In this case, the tests are carried out separately for the material and separately using it as finishes and facings.
6.6. For laminates with different surface layers, make two sets of specimens (according to 6.1) in order to expose both surfaces. In this case, the flammability group of the material is set according to the worst result.
6.7. Before testing, the samples are conditioned to achieve constant weight at a temperature of 23 ± 2 °C and a relative humidity of 50 ± 5%. Mass constancy is considered achieved if, during two successive weighings with an interval of 24 hours, the difference in the mass of the samples is no more than 0.1% of the initial mass of the sample.

7. Equipment for testing

7.1. General provisions
7.1.1. A general view of the flammability test facility is shown in Figure A1.
The installation consists of the following main parts:
- base frame;
- mobile platform;
- source of radiant heat flow (radiation panel);
- ignition system (auxiliary stationary burner, mobile burner with mechanized and manual movement system).
7.1.2. Auxiliary equipment includes: a sample holder, a shielding plate, a holder with a simulator sample, a gas-air mixture flow control system, regulating and recording devices, a heat flow and time meter.
7.1.3. The unit must be equipped with a protective screen and an exhaust hood.
7.1.4. All dimensions given in the following description of the installation, as well as in the figures, are nominal, except for those indicated with tolerances.

7.2. Base frame

7.2.1. The design of the support frame, the main components and details of the moving platform moving system are shown in Figures A2 and A3.
7.2.2. The base of the supporting frame is made in the form of a rectangular frame 275x230 mm in size from a 25x25 mm square profile with a wall thickness of 1.5 mm.
Four vertical supports with a diameter of 16 mm are mounted at the corners of the frame for attaching the protective plate. The distance from the frame to the protective plate is 260 mm.
7.2.3. The protective plate has the shape of a square with a side of 220 mm, the thickness of the plate is 4 mm. A hole with a diameter of 150 mm is cut out in the center of the protective plate. Along the edge of the hole on the upper side of the plate, a chamfer is cut at an angle of 45 ° with a size of 4 mm.
7.2.4. The movable platform for the sample has the shape of a square with a side of 180 mm, the thickness of the platform is 4 mm. A vertical rod with a boss at the lower end of the rod is installed in the center of the bottom side of the platform. Rod diameter - 12 mm, length 148 mm.
7.2.5. The system for moving the movable platform consists of two vertical guides (rods with a length of at least 355 mm and a diameter of 20 mm), a horizontal movable bar (section 25x25 mm) with two bushings at the ends of the bar and a hole in the center for the vertical rod of the movable platform, as well as counterweight lever.
7.2.6. Vertical guides are mounted in the center of the short sides of the frame (base of the support frame).
The horizontal movable bar is mounted on vertical rails. The bushings must ensure free movement of the bar along the guides. The position of the bar is fixed manually using screws.
A lever with a counterweight is installed under the horizontal bar. The lever should end with a roller resting against the boss of the vertical rod of the movable platform.
7.2.7. The lever with a counterweight must ensure the movement of the platform with the sample to the protective plate until a tight contact of the surface of the sample and the protective plate is achieved. These requirements are met by a lever with a length of approximately 320 mm with a counterweight of approximately 3 kg.
During melting, softening or shrinkage of the sample, the platform is allowed to move relative to the protective plate by a distance of not more than 5 mm. To meet this requirement, install an adjustable stop or use gaskets of non-combustible material placed between the platform and the protective plate.

7.3. Radiation panel

7.3.1. The radiation panel (Figures A4, A5) must provide the levels of exposure to radiant heat flux specified by the standard in the center of the opening of the protective plate, in a plane coinciding with its lower surface.
7.3.2. The radiation panel is installed on the vertical guides of the support frame. In this case, the distance from the lower edge of the radiation panel to the upper plane of the protective plate should be 22 ± 1 mm.
7.3.3. The radiation panel consists of a casing with a heat-insulating layer and a heating element. A non-combustible mineral fiber material is used as a heat-insulating layer.
7.3.4. A heating element with a diameter of 8 to 10 mm and a length of approximately 3.5 m (rated power 3 kW) is rolled up in the form of a truncated cone and attached to the inner surface of the casing.
7.3.5. Two thermoelectric converters are installed on the surface of the heating element at two diametrically opposite points. Each of them is attached to the coil of the heating element at a distance of 1/3 to 1/2 of the height of the casing of the radiation panel from its upper edge.
The fastening method should ensure tight contact of thermoelectric converters with the surface of the heating element. One of the recommended mounting methods is shown in Figure A5.
One of the thermoelectric converters is used to control the temperature of the heater (regulating thermoelectric converter), the second is used to control the temperature of the heater (controlling thermoelectric converter).

7.4. Ignition system

7.4.1. The movable burner must move from its initial position above the radiant panel to its working position inside the panel. The design of the movable burner and the system of its movement are shown in Figures A6 - A8.
7.4.2. The auxiliary burner is designed to ignite the mobile burner in the event of its extinction. The auxiliary burner nozzle has a diameter of 1 to 2 mm.
7.4.3. In the working position, the torch of the flame of the mobile burner must be located above the center of the hole in the protective plate in a plane perpendicular to the direction of movement of the burner. In this case, the center of the burner nozzle should be located at a distance of 10 ± 1 mm from the plane of the movable plate.
7.4.4. The movable burner must move from the starting position to the working position every 4 +0.4 s. The time spent by the burner in the working position should be 1 s.

7.5. Auxiliary equipment

7.5.1. The sample holder is a flat metal sheet, on the upper surface of which there are flanges for placing and fixing the sample (Figure A9). On the bottom surface of the holder there are guides and a stopper that fixes the position of the holder.
7.5.2. The shielding plate (Figure A10) is designed to protect the surface of the sample from the effects of heat flow. The shielding plate is made of 2 mm thick aluminum or stainless steel sheet.
7.5.3. The dummy specimen is made of non-combustible mineral fiber material with a density of 200±50 kg/m³ (Figure A11). The simulator sample holder is made of non-combustible material with a density of 825±125 kg/m³.
7.5.4. The gas-air mixture flow control system (Figure A12) is connected to sources of gaseous fuel (propane or propane-butane mixture) and air, contains needle valves, flow meters with an upper measurement limit of at least 1.2 l / h (for gas) and at least 12 l/h (for air) with an error of no more than 4%. It is also recommended to place filters on the fuel and air supply lines to protect the flow meters from impurities.
7.5.5. The device that regulates the temperature of the heating element of the radiant panel must be designed for a power of at least 3 kW and a current of at least 15 A. To record the temperature, it is recommended to use a device with an accuracy class of at least 0.5.
7.5.6. To measure PPTP, it is recommended to use a device with a measurement range of 1 to 75 kW / m², measurement error - no more than 5%. To register the readings of the heat flux meter, a recording device with an accuracy class of at least 0.1 is used.
7.5.7. As a time recorder, it is recommended to use devices with a measurement range of up to 1 hour, the measurement error should be no more than 1 s.
7.5.8. The installation location is equipped with protective screens and exhaust ventilation (Figure A13). An air flow reflector is installed in the exhaust hood, providing air speed in the gaps from 2 to 3 m/s at an air flow rate of 0.25 to 0.35 m³/s.

8. Installation calibration

8.1. General provisions
8.1.1. The purpose of calibration is to establish the values ​​of the FTDR required by this standard in accordance with 4.2, as well as the uniformity of its distribution within the exposed surface of the sample.
8.1.2. Uniform distribution of the heat flux over the exposed surface of the sample is ensured under the following conditions:
- deviation of PPTP at any four diametrically opposite points of a circle with a diameter of 50 mm from the value of PPTP in the center of the exposed surface should be no more than ± 3%;
- deviation of PPTP at any four diametrically opposite points of a circle with a diameter of 100 mm from the value of PPTP in the center of the exposed surface should be no more than ± 5%.
8.1.3. Establishment of the values ​​required by the standard PPTP is carried out by determining the dependence of PPTP in the center of the exposed surface on the temperature of the heating element.
8.1.4. Calibration is carried out on samples (3 pieces), having the shape of a square, with a side of 165 mm and a deviation of minus 5 mm. The thickness of the calibration specimen must be at least 20 mm. For the manufacture of a calibration sample, asbestos-cement sheets are used according to GOST 18124.
A hole is cut out in the calibration samples for installing a heat flux meter: in the first sample - in the center, in the second sample - at any point on a circle with a diameter of 50 mm, in the third sample - at any point on a circle with a diameter of 100 mm.
8.1.5. Calibration is carried out during metrological certification of the installation or replacement of the heating element and/or thermoelectric converters.

8.2. Calibration procedure

8.2.1. During calibration, the movable burner must be in its original position, the valves of the fuel and air supply system are closed.
8.2.2. Install the heat flow meter in the calibration sample with a hole in the center of the exposed surface.
8.2.3. The calibration sample is placed in the holder and placed on the movable platform.
8.2.4. It is turned on and by changing the power supplied to the heating element of the radiation panel, the value of thermoelectric power is selected using the regulating thermoelectric converter, at which a heat flux with a density of 50 kW/m² is provided in the center of the exposed surface.
8.2.5. Withstand the installation in the heating mode according to 8.2.4 for at least 10 min and fix the thermoEMF value of the controlling thermoelectric converter.
8.2.6. The operations according to 8.2.4, 8.2.5 are repeated in order to determine the thermoEMF values ​​that provide heat fluxes with a density of 45, 40, 35, 30, 25, 20, 10, 5 kW/m² in the center of the exposed surface.
8.2.7. After completing the operations in 8.2.6, install the heat flux meter in a calibration sample with a hole on a circle with a diameter of 50 mm and repeat the operations in 8.2.3 - 8.2.5 for heat fluxes with a density of 50, 40, 30, 20, 10 kW/m².
These measurements are repeated for each of the four diametrically opposite points of the circle, changing the position of the sample in the holder.
8.2.8. Repeat the calibration procedure of 8.2.7 on a calibration block with a hole on a circle with a diameter of 100 mm.
8.2.9. If the measurement results of the PPTP do not comply with the requirements of 8.1.2, the heating element of the radiation panel should be replaced.
8.2.10. The calibration control of the installation is carried out every 60 hours of operation of the radiation panel by the value of PPTP, equal to 30 kW/m², in the center of the exposed surface.
The calibration of the installation is repeated if the deviation of the measured value of the FTAP is more than 0.06 kW/m².

9. Testing

9.1. The test specimen, conditioned in accordance with 6.7, is wrapped in a sheet of aluminum foil (nominal thickness 0,2 mm) with a hole 140 mm in diameter cut in the center. In this case, the center of the hole in the foil should coincide with the center of the exposed surface of the sample (Figure A14).
9.2. The test specimen is placed in the holder, placed on the movable platform and the counterweight is adjusted. After that, the holder with the test sample is replaced by the holder with the dummy sample.
9.3. Set the movable burner to its original position according to 7.4.1, adjust the flow rate of gas (19 - 20 ml/min) and air (160 - 180 ml/min) supplied to the movable burner. For the auxiliary burner, the length of the flame is approximately 15 mm.
9.4. The power supply is switched on and the thermoelectric power value set during the calibration, corresponding to PPTP 30 kW/m², is set using the control thermoelectric converter.
9.5. After reaching the set thermoEMF value, the installation is maintained in this mode for at least 5 minutes. In this case, the thermoEMF value, recorded by the controlling thermoelectric converter, should differ from that obtained during calibration by no more than 1%.
9.6. Place the shield plate on the protective plate, replace the dummy piece with the test piece, turn on the movable burner mechanism, remove the shield plate, and turn on the time recorder.
The time for these operations should be no more than 15 s.
9.7. After 15 min or when the specimen ignites, the test is terminated. To do this, place the shielding plate on the protective plate, stop the time recorder and the mechanism of the movable burner, remove the holder with the sample and place the simulator sample on the movable platform, remove the shielding plate.
9.8. Set the value of PPTP 20 kW/m² if ignition was detected in the previous test, or 40 kW/m² if it was not. Repeat steps 9.5 - 9.7.
9.9. If ignition is detected at PPTP 20 kW/m², reduce the value of PPTP to 10 kW/m² and repeat steps 9.5 - 9.7.
9.10. If there is no ignition at TPDP 40 kW/m², set the TPDP value to 50 kW/m² and repeat steps 9.5 to 9.7.
9.11. After determining the two values ​​of APPF, at one of which ignition is observed, and at the other, there is no ignition, the value of APPF is set to 5 kW/m² more than the value at which ignition is absent, and the operations of 9.5 - 9.7 are repeated on three samples.
If ignition is detected at 10 kW/m² FTAP, then the following test is carried out at 5 kW/m² FTAP.
9.12. Depending on the results of the tests in 9.11, the value of the FTDR is increased by 5 kW/m² (in the absence of ignition) or reduced by 5 kW/m² (in the presence of ignition) and the operations of 9.5 - 9.7 are repeated on two samples.
9.13. For each tested sample, the ignition time and the following additional observations are recorded: time and place of ignition; the process of destruction of the sample under the action of thermal radiation and flame; melting, swelling, delamination, cracking, swelling or shrinkage.
9.14. For materials with high compressibility (mineral wool boards), as well as materials that melt or soften during heating, the test should be carried out taking into account 7.2.7.
9.15. For materials that acquire the ability to stick when heated, or form a surface charred layer with low mechanical strength, or contain an air gap under the exposed surface, in order to prevent interference with the movement of the movable burner or damage by the burner to the exposed surface of the sample, tests should be carried out using a stopper in the drive mechanism, eliminating the possibility of contact of the movable burner with the surface of the sample.
9.16. For materials that produce a significant amount of smoke or decomposition products, extinguishing the flame of the mobile burner and precluding the possibility of re-igniting it with the help of an auxiliary burner, the result is recorded in the test report indicating the absence of ignition due to the systematic extinguishing of the flame of the mobile burner by decomposition products.

10. Test report

The test report provides the following data:
- name of the testing laboratory;
- name of the customer;
- name of the manufacturer (supplier);
- description of the material or product, technical documentation, as well as the trade mark, composition, thickness, density, mass and method of manufacturing samples, characteristics of the exposed surface, for layered materials - the thickness of each layer and the characteristics of the material of each layer;
- flammability parameters: APPT, ignition time at APPT for each of the samples;
- conclusion about the flammability group of the material, indicating the value of KPPTP;
- additional observations when testing the sample: time and place of ignition; the process of destruction of the sample under the action of thermal radiation and flame; melting, swelling, delamination, cracking, swelling or shrinkage.

11. Safety requirements

The room in which the tests are carried out must be equipped with supply and exhaust ventilation. The operator's workplace must meet the electrical safety requirements in accordance with GOST 12.1.019 and the sanitary and hygienic requirements in accordance with GOST 12.1.005.

APPENDIX A (informative)

Dimensions in mm
Figure A2 - Support frame (section BB)
1 - radiation panel with a heating element; 2 - movable burner; 3 - auxiliary stationary burner; 4 - power cable of the heating element; 5 - cam with stroke limiter for manual control of a movable burner; 6 - cam for automatic control of a movable burner; 7 - drive belt; 8 - sleeve for connecting a movable burner to the fuel supply system; 9 - mounting plate for the ignition system and the system for moving the movable burner; 10 - protective plate; 11 - vertical support; 12 - vertical guide; 13 - movable platform for the sample; 14 - the base of the support frame; 15 - manual control; 16 - lever with counterweight; 17 - drive to the electric motor
1 - radiation panel; 2 - protective plate; 3 - mobile platform; 4 - counterweight; 5 - lever



Detail 5 Detail 6
1 - casing with a heat-insulating layer; 2 - heat-insulating layer of mineral fiber; 3 - heating element; 4 - clamp; 5 - thermoelectric converter
1 - sleeve for connecting a movable burner to the fuel supply system; 2 - flexible hose; 3 - counterweight; 4 - roller; 5 - nozzle; 6 - flame stabilizer
Figure A6 - Movable burner
1 - shaft of the drive mechanism; 2 - cam drive mechanism; 3 - cam with stroke limiter; 4 - manual control shaft; 5 - line passing through the center of the radiation panel
Figure A7 - Mounting plate for mobile burner handling system
1 - cam drive mechanism; 2 - cam with stroke limiter
Figure A8 - Movable burner drive mechanism (mesh with a square side of 10 mm)
1 - rivets; 2 - handle; 3 - metal sheet (thickness 0.7)
Figure A9 - Sample holder
1 - flat sheet of aluminum or stainless steel (thickness 2 mm); 2 - handle; 3 - rivets
Figure A10 - Shielding plate

1 - mineral fiber plate; 2 - corner post with self-tapping screw; 3 - the base of the simulator sample; 4 - handle
1 - temperature controller; 2 - connection of thermocouples; 3 - power supply; 4 - millivoltmeter; 5 - heat flow meter; 6 - radiation panel; 7 - movable burner; 8 - auxiliary burner; 9 - sleeve for connecting a movable burner to the fuel supply system; 10 - non-return valves; 11 - needle valve; 12 - gearbox; 13 - flow meters; 14 - filters; 15 - needle valves; 16 - reducers-pressure regulators; 17 - compressed air supply; 18 - propane

1 - reflector; 2 - gap (along all edges of the reflector); 3 - protective screens
1 - aluminum foil; 2 - sample

Key words: building materials, flammability, testing, flammability group, combustible materials, critical heat flow surface, ignition time

BUILDING MATERIALS

GOST R

STATE STANDARD OF THE RUSSIAN FEDERATION

BUILDING MATERIALS

FLAME PROPAGATION TEST METHOD

GOST R

BUILDING MATERIALS

SPREAD FLAME TEST METHOD

Introduction date 1997-01-01

Introduction

This International Standard has been developed on the basis of draft ISO/IMS 9239.2 “Basic tests - Reaction to fire - Spread of flame over a horizontal surface of floor coverings by a radiant thermal ignition source”.

Sections 6 to 8 of this International Standard are authentic to the corresponding sections of draft ISO/IMS 9239.2.

1 area of ​​use

This International Standard establishes a test method for the spread of flames on the materials of the surface layers of floor and roof structures, as well as their classification into flame spread groups.

This International Standard applies to all homogeneous and layered combustible building materials used in the surface layers of floor and roof structures.

GOST 12.1.005-88 SSBT. General sanitary and hygienic requirements for the air of the working area

GOST 12.1.019-79 SSBT. Electrical safety. General requirements and nomenclature of types of protection

GOST 3044-84 Thermoelectric converters. Rated static conversion characteristics

GOST 18124-95 Flat asbestos-cement sheets. Specifications


GOST 30244-94 Construction materials. Flammability test methods

The capacity of the exhaust fan must be at least 0.5 m3/s.

7.4 The radiation panel has the following dimensions:

length................................................. .................±10) mm;

width................................................. ..............±10) mm.

The electrical power of the radiation panel must be at least 8 kW.

The angle of inclination of the radiation panel (Figure 2) to the horizontal plane should be (30±5) °.

7.5 The source of ignition is a gas burner with an outlet diameter of (1.0 ± 0.1) mm, which ensures the formation of a flame torch with a length of 40 to 50 mm. The design of the burner must ensure the possibility of its rotation about the horizontal axis. During testing, the flame of the gas burner should touch the “zero” (“0”) point of the longitudinal axis of the sample (Figure 2).

Dimensions are given for reference in mm

1 - holder; 2 - sample; 3 - radiation panel; 4 - gas-burner

Figure 2 - Scheme of mutual arrangement of the radiation panel, sample and gas burner

7.6 The platform for placing the sample holder is made of heat-resistant or stainless steel. The platform is mounted on rails in the lower part of the chamber along its longitudinal axis. Along the entire perimeter of the chamber between its walls and the edges of the platform, a gap with a total area of ​​(0.24 ± 0.04) m2 should be provided.

The distance from the exposed sample surface to the ceiling of the chamber should be (710 ± 10) mm.

7.7 The sample holder is made of heat-resistant steel with a thickness of (2.0 ± 0.5) mm and is equipped with devices for fixing the sample (Figure 3).

1 - holder; 2 - fasteners

Figure 3- Sample holder

7.8 To measure the temperature in the chamber (Figure 1), a thermoelectric transducer is used according to GOST 3044 with a measurement range from 0 to 600 °C and a thickness of not more than 1 mm. To register the readings of a thermoelectric converter, devices with an accuracy class of not more than 0.5 are used.

7.9 To measure PPTP, water-cooled thermal radiation receivers with a measurement range of 1 to 15 kW/m2 are used. The measurement error should be no more than 8%.

To register the readings of the thermal radiation receiver, a recording device with an accuracy class of not more than 0.5 is used.

7.10 To measure and record the air flow velocity in the chimney, anemometers are used with a measurement range of 1 to 3 m/s and a basic relative error of not more than 10%.

8 Installation calibration

8.1 General

8.1.1 The purpose of calibration is to establish the values ​​of the FTDR required by this standard at the control points of the calibration sample (Figure 4 and Table 2) and the distribution of the FTDR over the surface of the sample at an air flow velocity in the chimney of (1.22 ± 0.12) m / s.

table 2

8.1.2 Calibration is carried out on a sample made of asbestos-cement sheets according to GOST 18124, with a thickness of 10 to 12 mm (Figure 4).

1 - calibration sample; 2 - holes for heat flow meter

Figure 4 - Calibration sample

8.1.3 Calibration is carried out during metrological certification of the installation or replacement of the heating element of the radiation panel.

8.2 Calibration procedure

8.2.1 Set the air flow rate in the chimney from 1.1 to 1.34 m/s. To do this, do the following:

An anemometer is placed in the chimney so that its inlet is located along the axis of the chimney at a distance of (70 ± 10) mm from the upper edge of the chimney. The anemometer should be rigidly fixed in the installed position;

Fix the calibration sample in the sample holder and install it on the platform, insert the platform into the chamber and close the door;

The air flow rate is measured and, if necessary, by adjusting the air flow in the ventilation system, the required air flow rate in the chimney is set in accordance with 8.1.1, after which the anemometer is removed from the chimney.

At the same time, the radiation panel and the gas burner are not included.

8.2.2 After carrying out the work according to 8.2.1, the values ​​​​of the PPTP are set in accordance with table 2. For this purpose, the following is performed:

The radiation panel is turned on and the chamber is heated until the thermal balance is reached. The heat balance is considered achieved if the temperature in the chamber (Figure 1) changes by no more than 7 ° C within 10 minutes;

Installed in the hole of the calibration sample at the control point L2(Figure 4) thermal radiation receiver so that the surface of the sensitive element coincides with the upper plane of the calibration sample. The readings of the thermal radiation receiver are recorded after (30 ± 10) s;

If the measured value of PPTP does not meet the requirements specified in Table 2, adjust the power of the radiation panel to achieve heat balance and repeat the measurement of PPTP;

The above operations are repeated until the value of the FTAP required by this standard for the control point is reached. L2.

8.2.3 The operations in 8.2.2 are repeated for control points. L1, and l3(Figure 4). If the measurement results comply with the requirements of Table 2, PPTP measurements are carried out at points located at a distance of 100, 300, 500, 700, 800 and 900 mm from the “0” point.

Based on the results of the calibration, a graph of the distribution of the values ​​of PPTP along the length of the sample is plotted.

9 Testing

9.1 Preparation of the installation for testing is carried out in accordance with 8.2.1 and 8.2.2. After that, the chamber door is opened, the gas burner is ignited and positioned so that the distance between the flame and the exposed surface is at least 50 mm.

9.2 Install the sample in the holder, fix its position with the help of fasteners, place the holder with the sample on the platform and enter into the chamber.

9.3 Close the chamber door and start the stopwatch. After holding for 2 minutes, the burner flame is brought into contact with the sample at the “0” point located along the central axis of the sample. Leave the flame in this position for (10 ± 0.2) min. After this time, return the burner to its original position.

9.4 If the sample does not ignite within 10 min, the test is considered to be completed.

If the sample ignites, the test is terminated when the flame combustion ceases or after 30 minutes from the start of exposure to the gas burner sample by forced extinguishing.

During the test, the ignition time and the duration of flame burning are recorded.

9.5 After the end of the test, the chamber door is opened, the platform is pulled out, and the sample is removed.

The test of each subsequent sample is carried out after the sample holder has cooled to room temperature and compliance with the FTAP at the point L2 the requirements specified in table 2.

9.6 Measure the length of the damaged part of the sample along its longitudinal axis for each of the five samples. Measurements are carried out with an accuracy of 1 mm.

Damage is considered to be burnout and charring of the sample material as a result of the spread of fiery combustion over its surface. Melting, warping, sintering, swelling, shrinkage, change in color, shape, violation of the integrity of the sample (tears, surface chips, etc.) are not damage.

10 Processing of test results

10.1 The length of flame propagation is determined as the arithmetic mean of the length of the damaged part of the five samples.

10.2 The value of PPDC is set on the basis of the results of measuring the length of flame propagation (10.1) according to the plot of the distribution of PPDC over the surface of the sample, obtained during the calibration of the installation.

10.3 In the absence of ignition of the specimens or the flame propagation length is less than 100 mm, it should be considered that the material's CTF is more than 11 kW/m2.

10.4 In the case of forced extinguishing of the sample after 30 minutes of testing, the value of PPTP is determined by the results of measuring the flame propagation length at the moment of extinguishing and conditionally take this value equal to the critical one.

10.5 For materials with anisotropic properties, the smallest of the obtained values ​​of the CTP is used in the classification.

11 Test report

The test report provides the following data:

Name of the testing laboratory;

Name of the customer;

Name of the manufacturer (supplier) of the material;

Description of the material or product, technical documentation, as well as the trademark, composition, thickness, density, mass and method of manufacturing samples, characteristics of the exposed surface, for layered materials - the thickness of each layer and the characteristics of the material of each layer;

Flame propagation parameters (flame propagation length, KPPTP), as well as the ignition time of the sample;

Conclusion on the distribution group of the material, indicating the value of the KPPTP;

Additional observations during testing of the sample: burnout, charring, melting, swelling, shrinkage, delamination, cracking, as well as other special observations during flame propagation.

12 Safety requirements

The room in which the tests are carried out must be equipped with supply and exhaust ventilation. The operator's workplace must meet the electrical safety requirements in accordance with GOST 12.1.019 and the sanitary and hygienic requirements in accordance with GOST 12.1.005.

Keywords: building materials, flame propagation, surface heat flux density, critical heat flux density, flame propagation length, test specimens, test chamber, radiation panel

INTRODUCED Office of Standardization, Technical Regulation and Certification of the Ministry of Construction of Russia

The standard establishes a method for testing the spread of flame on the materials of the surface layers of floor and roof structures, as well as classifying them into groups of flame propagation. This standard applies to all homogeneous and layered combustible building materials used in the surface layers of floor and roof structures.

Designation: GOST 30444-97
Russian name: Construction materials. Flame propagation test method
Status: valid
Text update date: 05.05.2017
Date added to database: 12.02.2016
Date of entry into force: 20.03.1998
Approved: 03/20/1998 Gosstroy of Russia (Russian Federation Gosstroy 18-21) 04/23/1997 Interstate Scientific and Technical Commission for Standardization and Technical Regulation in Construction (MNTKS)
Published: GUP TsPP (CPP GUP 1998)
Download links:

GOST R51032-97

STATE STANDARD OF THE RUSSIAN FEDERATION

BUILDING MATERIALS

TEST METHOD
FLAME DISTRIBUTION

MINSTROY OF RUSSIA

Moscow

Foreword

1 DEVELOPED by the State Central Research and Design and Experimental Institute of Complex Problems of Building Structures and Structures. V. A. Kucherenko (TsNIISK named after Kucherenko) of the State Scientific Center "Construction" (SSC "Construction"), All-Russian Research Institute of Fire Protection (VNIIPO) of the Ministry of Internal Affairs of Russia with the participation of the Moscow Institute of Fire Safety of the Ministry of Internal Affairs of Russia

INTRODUCED by the Office of Standardization, Technical Regulation and Certification of the Ministry of Construction of Russia

2 ADOPTED and put into effect by the Decree of the Ministry of Construction of Russia dated December 27, 1996 No. 18-93

Introduction

This International Standard has been developed from ISO/IMS 9239.2 Basic Tests - Reaction to Fire - Flame Propagation on a Horizontal Surface of Floor Coverings by a Radiant Thermal Ignition Source.

Dimensions are given for reference in mm

1 - test chamber; 2 - platform; 3 - sample holder; 4 - sample; 5 - chimney;
6 - exhaust umbrella; 7 - thermocouple; 8 - radiation panel; 9 - gas-burner;
10 - viewing window door

Picture 1 - Flame Propagation Tester

The installation consists of the following main parts:

1) test chamber with chimney and exhaust hood;

2) source of radiant heat flow (radiation panel);

3) ignition source (gas burner);

4) sample holder and a device for inserting the holder into the test chamber (platform).

The installation is equipped with devices for recording and measuring the temperature in the test chamber and flue, the value of the surface heat flux density, the air flow velocity in the chimney.

7.2 The test chamber and flue () are made of sheet steel with a thickness of 1.5 to 2 mm and are lined from the inside with a non-combustible heat-insulating material with a thickness of at least 10 mm.

The front wall of the chamber is equipped with a door with a viewing window made of heat-resistant glass. The size of the viewing window should allow observation of the entire surface of the sample.

7.3 The chimney is connected by a scammer through an opening. An exhaust ventilation hood is installed above the chimney.

The capacity of the exhaust fan must be at least 0.5 m3/s.

7.4 Radiation panel has the following dimensions:

The electrical power of the radiation panel must be at least 8 kW.

The angle of inclination of the radiation panel () to the horizontal plane should be (30 ± 5) °.

7.5 The ignition source is a gas burner with an outlet diameter of (1.0 ± 0.1) mm, which ensures the formation of a flame torch with a length of 40 to 50 mm. The design of the burner must ensure the possibility of its rotation relative to the horizontal axis. When testing, the flame of a gas burner should touch the "zero" ("0") point of the longitudinal axis of the sample ().

Dimensions are given for reference in mm

1 - holder; 2 - sample; 3 - radiation panel; 4 - gas-burner

Figure 2 - Scheme of the relative position of the radiation panel,
sample and gas burner

7.6 The platform for placing the sample holder is made of heat-resistant or stainless steel. The platform is installed on rails in the lower part of the chamber along its longitudinal axis. A gap with a total area of ​​(0.24 ± 0.04) m 2 should be provided around the entire perimeter of the chamber between its walls and the edges of the platform.

The distance from the exposed surface of the specimen to the ceiling of the chamber shall be (710 ± 10) mm.

7.7 The sample holder is made of heat-resistant steel with a thickness of (2.0 ± 0.5) mm and equipped with fixtures for holding the sample ().

1 - holder; 2 - fasteners

Figure 3 - Sample holder

7.8 To measure the temperature in the chamber (), use a thermoelectric converter according to GOST 3044 with a measurement range from 0 to 600 ° C and a thickness of not more than 1 mm. To register the readings of a thermoelectric converter, devices with an accuracy class of not more than 0.5 are used.

7.9 To measure PPTP, water-cooled thermal radiation receivers with a measurement range of 1 to 15 kW/m 2 are used. The measurement error should be no more than 8%.

To register the readings of the thermal radiation receiver, a recording device with an accuracy class of not more than 0.5 is used.

7.10 To measure and record the air flow velocity in the chimney, anemometers with a measurement range of 1 to 3 m/s and a basic relative error of no more than 10% are used.

8 Installation calibration

8.1 General

9.6 Measure the length of the damaged part of the sample along its longitudinal axis for each of the five samples. Measurements are carried out with an accuracy of 1 mm.

Damage is considered to be burnout and charring of the sample material as a result of the spread of fiery combustion over its surface. Melting, warping, sintering, swelling, shrinkage, change in color, shape, violation of the integrity of the sample (tears, surface chips, etc.) are not damage.

10 Processing of test results

10.1 The length of flame propagation is determined as the arithmetic mean of the length of the damaged part of the five samples.

10.2 The value of PPTP is established on the basis of the results of measuring the flame propagation length (10.1) according to the plot of PPTP distribution over the surface of the sample, obtained by calibrating the installation.

10.3 If the specimens do not ignite or if the flame propagation length is less than 100 mm, the material should be considered to have a CDP of more than 11 kW/m 2 .

10.4 In the case of forced extinguishing of the sample after 30 minutes of the test, the value of the flame resistance is determined by the results of measuring the flame propagation length at the moment of extinguishing and conditionally take this value equal to the critical one.

10.5 For materials with sanitary-isotropic properties, the smallest of the obtained values ​​of the CPP is used in the classification.

11 Test report

The test report contains the following information:

Name of the testing laboratory;

Name of the customer;

Name of the manufacturer (supplier) of the material;

Description of the material or product, technical documentation, as well as the trade mark, composition, thickness, density, mass and method of manufacturing samples, characteristics of the exposed surface, for layered materials - the thickness of each layer and the characteristics of the material of each layer;

Flame propagation parameters (flame propagation length, KPPTP), as well as the ignition time of the sample;

Conclusion on the distribution group of the material, indicating the value of the KPPTP;

Additional observations when testing a sample: burnout, charring, melting, swelling, shrinkage, delamination, cracking, as well as other special observations during flame propagation.

12 Safety requirements

The room in which the tests are carried out must be equipped with supply and exhaust ventilation. The operator's workplace must meet the electrical safety requirements in accordance with GOST 12.1.019 and the sanitary and hygienic requirements in accordance with GOST 12.1.005.

Keywords: building materials , flame spread , surface heat flux density , critical heat flux density , flame propagation length , samples for testing , test chamber , radiation panel

Moderately flammable (B2), having a critical surface heat flux density of at least 20, but not more than 35 kilowatts per square meter;

Flammable (B1), having a critical surface heat flux density of more than 35 kilowatts per square meter;

Highly combustible (G4), having a flue gas temperature of more than 450 degrees Celsius, the degree of damage along the length of the test sample is more than 85 percent, the degree of damage by weight of the test sample is more than 50 percent, the duration of independent combustion is more than 300 seconds.

Normally combustible (G3), having a flue gas temperature of not more than 450 degrees Celsius, the degree of damage along the length of the test sample is more than 85 percent, the degree of damage by weight of the test sample is not more than 50 percent, the duration of independent combustion is not more than 300 seconds;

Moderately combustible (G2), having a flue gas temperature of not more than 235 degrees Celsius, the degree of damage along the length of the test sample is not more than 85 percent, the degree of damage by weight of the test sample is not more than 50 percent, the duration of independent combustion is not more than 30 seconds;

Slightly combustible (G1), having a flue gas temperature of not more than 135 degrees Celsius, the degree of damage along the length of the test sample is not more than 65 percent, the degree of damage by weight of the test sample is not more than 20 percent, the duration of self-burning is 0 seconds;

Combustible - substances and materials capable of spontaneous combustion, as well as ignite under the influence of an ignition source and burn independently after its removal.

Slow-burning - substances and materials capable of burning in air when exposed to an ignition source, but unable to burn independently after its removal;